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Rhodium(I)-Catalyzed Cascade Annulation of 1,n-Diynyl Nitrones to 3,4-Fused Fully Substituted Furans

Abbate, Sergio1; Test, Kevin1

Published Oct 31, 2024 on Dryad. https://doi.org/10.7959/dryad.dz08kprt4

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Oct 31, 2024 version files 705 B

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Abstract

A method for the assembly of fully substituted furans containing a 3,4-fused 5–8 membered carbocycle, heterocycle, or spirocycle from rhodium(I)-catalyzed and 1,1,1,3,3,3-hexafluoroisopropanol (HFIP)-assisted cascade annulation of 1,n-diynyl nitrones has been developed.